Factors influencing paper chromatographic analysis of technetium-99m phosphorus compounds: concise communication.
A single-paper chromatographic system has been developed, capable of resolving Tc-99m dioxide, [99mTc] pertechnetate and Tc-99m phosphorus compounds. The best separations are obtained with CM82 paper developed in 0.5 m naCl, and 3MM or ashless No. 40 paper developed in 1 M sodium acetate buffer. In these systems, 99TcO2 remains at the origin, while 99mTcO4--and Tc-99m phosphorus compounds move with Rf values of 0.56--0.75 and 0.80--1.0, respectively.
D002854:Chromatography, Paper / Q000379:methods; D011756:Diphosphates / Q000032:analysis*; D004164:Diphosphonates / Q000032:analysis*; D011877:Radionuclide Imaging / Q000592:standards; D013667:Technetium / Q000032:analysis*
D011756:Diphosphates; D004164:Diphosphonates; D013667:Technetium