Analysis of bile acids in serum and bile by capillary gas-liquid chromatography.
Various liquid phases for glass capillary columns have been evaluated for gas-liquid chromatographic analysis of methyl ester trimethylsilylether derivatives of bile acids from serum and bile. Bile acid analysis is rapid and exhibits high separation efficiency with a 20 X 0.3 mm glass capillary column whose internal surface is covered with a crystal layer of barium carbonate and coated with polyethyleneglycol 20000 as liquid phase according to Grob et al.
D001646:Bile / Q000032:analysis*; D001647:Bile Acids and Salts / Q000097:blood*; D002849:Chromatography, Gas / Q000379:methods; D006801:Humans; D014297:Trimethylsilyl Compounds / Q000032:analysis
D001647:Bile Acids and Salts; D014297:Trimethylsilyl Compounds