Determination of terbacil in soil by gas-liquid chromatography with 63Ni electron capture detection.
A method is described for the determination of terbacil residue in soil. The herbicide residue is extracted with 1.5% NaOH, partitioned into an organic phase and subsequently cleaned up by passing through a Florisil column. Extract is analyzed by gas-liquid chromatography using a 63Ni electron capture detector. The procedure has a sensitivity of about 0.01 ppm, based on a 20 g sample. The method was used for the analysis of terbacil residues in the field treated soil samples.
D002849:Chromatography, Gas / Q000379:methods; D006540:Herbicides / Q000032:analysis*; D013058:Mass Spectrometry; D009532:Nickel; D011868:Radioisotopes; D012987:Soil / Q000032:analysis*; D014498:Uracil / Q000031:analogs & derivatives* / Q000032:analysis
D006540:Herbicides; D011868:Radioisotopes; D012987:Soil; D014498:Uracil; D009532:Nickel