Collaborative study of a gas-liquid chromatographic method for the analysis of propazine.
A gas-liquid chromatographic method for the determination of propazine in wettable powder formulations containing about 80% active ingredient was collaboratively studied, using a matched pair scheme. The propazine was extracted from the powder with chloroform, with dieldrin as an internal standard, and chromatographed on Carbowax 20M, using a flame ionization detector. Two samples were analyzed using peak height measurements with the following results (13 collaborators): 1.2% overall coefficient of variation and 1.2% coefficient of variation for the random error. Statistical evaluation of these factors reveals no evidence of systematic error contribution. The method has been adopted as official first action.
D002725:Chloroform; D002849:Chromatography, Gas; D008722:Methods; D011208:Powders / Q000032:analysis; D014227:Triazines / Q000032:analysis* / Q000592:standards
D011208:Powders; D014227:Triazines; D002725:Chloroform