Decomposition of 11-deoxycorticosterone and corticosterone in soda-lime glass.
When methanolic solutions of tritiated 11-deoxycorticosterone or corticosterone (0.1 to 300 ng) were evaporated to dryness with a stream of nitrogen in soda-lime test tubes only 8-24% of the radioactivity was recovered as the parent steroid. Evaporation in borosilicate test tubes led to a recovery of 90% or more. With ethyl acetate as solvent no decomposition occured in soda-lime test tubes.
D055598:Chemical Phenomena; D002621:Chemistry; D003345:Corticosterone; D003900:Desoxycorticosterone; D005898:Glass; D012997:Solvents; D014316:Tritium
D012997:Solvents; D014316:Tritium; D003900:Desoxycorticosterone; D003345:Corticosterone