[The identification and determination of marker substances in xiaoyao wan by three dimensional HPLC].
A Chinese traditional patent medicine Xiaoyao Wan was analysed by three dimensional HPLC. The result shows that the Chinese traditional medicines involved in Xiaoyao Wan were identified excellently and the content of marker substances can be determined accurately. According to the results of determination, the content of saikosaponin b1, b2, glycyrrhizin, paeoniflorin and atractylenolide III in Xiaoyao Wan was 0.43, 0.53, 5.22, 3.95 and 0.16 (mg/g), respectively; The RSD was 1.2, 0.8, 0.4, 0.3 and 1.0 (%) respectively.
Chen
F K
FK
Shenyang College of Pharmacy.
Meng
X S
XS
Guo
Y Z
YZ
Kano
Y
Y
D001565:Benzoates; D001952:Bridged-Ring Compounds; D002851:Chromatography, High Pressure Liquid / Q000379:methods; D004365:Drugs, Chinese Herbal / Q000737:chemistry*; D005960:Glucosides / Q000032:analysis*; D006034:Glycyrrhetinic Acid / Q000031:analogs & derivatives* / Q000032:analysis; D019695:Glycyrrhizic Acid; D039821:Monoterpenes; D009828:Oleanolic Acid / Q000031:analogs & derivatives*; D012502:Sapogenins / Q000032:analysis*; D012503:Saponins; D006027:Glycosides
D001565:Benzoates; D001952:Bridged-Ring Compounds; D004365:Drugs, Chinese Herbal; D005960:Glucosides; D006034:Glycyrrhetinic Acid; D019695:Glycyrrhizic Acid; D039821:Monoterpenes; D009828:Oleanolic Acid; D012502:Sapogenins; D012503:Saponins; C015423:peoniflorin; D006027:Glycosides; C025759:saikosaponin D