Presentation of sideband envelopes by two-dimensional one-pulse (TOP) spectroscopy.
A novel way of representing 1D MAS spinning sideband spectra in a 2D-resolved fashion is explained. The method is illustrated with 2H MAS data of deuterated polycarbonate. From the resulting 2D spectrum, the isotropic shifts can be identified on one axis and the rotary echo decay spectra along the other axis.
Blümich
B
B
Max-Planck-Institut für Polymerforschung, Mainz, Germany.
Blümler
P
P
Jansen
J
J
D003903:Deuterium / Q000737:chemistry; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D015394:Molecular Structure; D011076:Polycarboxylate Cement / Q000737:chemistry
D011076:Polycarboxylate Cement; C005506:polycarbonate; D003903:Deuterium