title: Determination of doughing and manipulation times of acrylic resin denture base material and a proposal for a specification for a packing plasticity test.
abstract: The doughing and manipulation times of a range of acrylic resin denture base polymers are presented in this study. The methods evaluated were: (i) probing following American Society for testing materials specification, F451-76; (ii) hole penetration following British Standard, 2487: 1989 and International Standard Organisation, 1567: 1988; (iii) probing using a penetrometer employing a 20 g load and 1 mm diameter needle; (iv) oscillating rheometer apparatus used at a fixed frequency of 1 Hz by sweeping through a programmed linear increase in strain. The results indicate that each of the methods is capable of evaluating the doughing and manipulation times of the unprocessed polymers. It is concluded that the Bohlin VOR Oscillating Rheometer is excellent for investigating the flow properties of denture base polymers but it cannot be recommended for a standards specification test because of the high cost. The penetrometer method has been shown to be superior to the current standards specification test and would be ideal for a packing plasticity standards test.
authors.affiliation: Department of Prosthetic Dentistry & Dental Care of the Elderly, University of Bristol Dental School, UK.
authors.forename: G
authors.initials: G
authors.lastname: Mutlu
authors.forename: R
authors.initials: R
authors.lastname: Huggett
authors.forename: A
authors.initials: A
authors.lastname: Harrison
mesh_terms: D003819:Denture Bases; D008422:Materials Testing / Q000295:instrumentation / Q000379:methods; D008689:Methacrylates; D020366:Methylmethacrylate; D008768:Methylmethacrylates / Q000737:chemistry; D008838:Microcomputers; D011109:Polymethacrylic Acids / Q000737:chemistry*; D012015:Reference Standards; D012212:Rheology; D013997:Time Factors; D014783:Viscosity
chemical_list: D008689:Methacrylates; D008768:Methylmethacrylates; D011109:Polymethacrylic Acids; D020366:Methylmethacrylate; C009931:poly(ethylmethacrylate); C016284:butyl methacrylate