[The determination of phoxim in cadaveric material by gas-liquid chromatography].
The developed gas-liquid chromatographic procedure for forensic chemical detection and measurement of phoxim in cadaveric material permits the detection in 25 g of an organ of 44 to 52% of added phoxim. The threshold of phoxim measurement in 100 g of the liver is 0.04 mg, the least volume of phoxim detectable being 0.02 g. The developed gas-liquid chromatographic technique should be used as an additional method together with thin-layer chromatography, for a more objective evaluation of the results of forensic chemical analysis of cadaveric material for phoxim.
Orlova
A M
AM
Salomatin
E M
EM
D002102:Cadaver; D002849:Chromatography, Gas / Q000295:instrumentation / Q000379:methods; D005554:Forensic Medicine / Q000379:methods; D006801:Humans; D007306:Insecticides / Q000032:analysis* / Q000302:isolation & purification; D008099:Liver / Q000737:chemistry; D009946:Organothiophosphorus Compounds / Q000032:analysis* / Q000302:isolation & purification; D012996:Solutions
D007306:Insecticides; D009946:Organothiophosphorus Compounds; D012996:Solutions; C003135:phoxim
Opredelenie foksima v trupnom materiale metodom gazozhidkostnoĭ khromaografii.