Determination of conditions for optimum resolution of a high angle thin window energy dispersive spectrometer.
The energy resolution of an energy dispersive spectrometer (EDS) equipped with an ultrathin window (UTW) and mounted at a high take-off angle (72 degrees) on a transmission electron microscope has been studied under a variety of operating conditions. The spectrometer resolution is close to that specified by the manufacturer, up to count rates of 400 cps. Above 400 cps the resolution deteriorates rapidly, and the MCA dead time and zero width increase. Above 10 keV, the height of the background is much greater than expected for bremsstrahlung and shows the shape which has previously been attributed to backscattered electron flux into the detector. It is postulated that the deterioration in resolution with count rate is caused by backscattered electrons reaching the detector through the UTW.
Blackford
M G
MG
Advanced Materials Program, Australian Nuclear Science and Technology Organisation, Menai, NSW.
Smith
K L
KL
D004577:Electron Probe Microanalysis / Q000379:methods* / Q000592:standards