1H and 13C-NMR assignments for sialylated oligosaccharide-alditols related to mucins. Study of thirteen components from hen ovomucin and swallow nest mucin.
Four hundred MHz 1H-NMR and 100 MHz 13C-NMR spectra of thirteen sialylated oligosaccharide-alditols isolated from hen ovomucin and swallow nests (Collocalia mucin) were studied. The resonance assignments were determined by combining multiple-relayed coherence-transfer chemical-shift-correlated spectroscopy (multiple-Relay-Cosy) and 1H/13C chemical-shift-correlated 2-D experiments.
Strecker
G
G
Université des Sciences et Techniques de Lille Flandres-Artois, Laboratoire de Chimie Biologique (UMR no 111 du CNRS) Villeneuve-d'Ascq, France.
Wieruszeski
J M
JM
Cuvillier
O
O
Michalski
J C
JC
Montreuil
J
J
D000818:Animals; D001717:Birds; D002247:Carbon Isotopes; D002645:Chickens; D009682:Magnetic Resonance Spectroscopy; D009077:Mucins / Q000032:analysis*; D009844:Oligosaccharides / Q000032:analysis*; D010059:Ovomucin / Q000032:analysis*; D014316:Tritium
D002247:Carbon Isotopes; D009077:Mucins; D009844:Oligosaccharides; D014316:Tritium; D010059:Ovomucin