Determination of degree of substitution of formyl groups in polyaldehyde dextran by the hydroxylamine hydrochloride method.
Colorimetric or potentiometric titration of the aldehyde residues in polyaldehyde dextran by the hydroxylamine hydrochloride/sodium hydroxide method has been found to be a convenient and accurate method to determine formyl content. Nitrogen combustion analyses on the isolated oximes confirmed the titrametric results.
Zhao
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Department of Chemistry, Lehigh University, Bethlehem, Pennsylvania 18015.
Heindel
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D000447:Aldehydes / Q000032:analysis; D003124:Colorimetry / Q000379:methods; D003911:Dextrans / Q000032:analysis*; D019811:Hydroxylamine; D006898:Hydroxylamines / Q000032:analysis; D009584:Nitrogen / Q000032:analysis; D011199:Potentiometry / Q000379:methods
D000447:Aldehydes; D003911:Dextrans; D006898:Hydroxylamines; D019811:Hydroxylamine; C026948:dextran dialdehyde; D009584:Nitrogen