[Use of high pressure liquid chromatography with diode array detector in "generally unknown" cases].
Procedures are described by general-unknown cases for the screening of drugs by reverse-phase high-pressure-liquid-chromatography (HPLC) with diode-array detector (DAD). The column is LiChrospher RP 18 (microbore column) and the mobile phase a mixtures of methanol/water, acetonitrile (ACN)/phosphate-buffer (pH 2.3) or ACN/H2SO4, 1-heptanosulfonic acid. Procedures are described for the work-out of spectren libraries with in each case c. 250 drugs and narcotic drugs for above mobile phases.
Felscher
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Institut für Gerichtliche Medizin, Medizinischen Akademie Carl Gustav Carus, Dresden.
D002851:Chromatography, High Pressure Liquid / Q000295:instrumentation*; D006801:Humans; D013287:Illicit Drugs / Q000032:analysis*; D004364:Pharmaceutical Preparations / Q000032:analysis*; D011619:Psychotropic Drugs / Q000032:analysis*; D012815:Signal Processing, Computer-Assisted / Q000295:instrumentation*
D013287:Illicit Drugs; D004364:Pharmaceutical Preparations; D011619:Psychotropic Drugs
Die Anwendung der Hochdruck-Flüssigkeitschromatographie mit Diodenarray-Detektor auf "general-unknown"-Fälle.