X-ray structure of the (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6- tetra-O-acetyl-beta-D-glucopyranoside.
The crystal structure of (2,2,6,6-tetramethylpiperidin-1-oxyl-4-yl)2,3,4,6-tetra-O-acetyl-b eta-D- glucopyranoside, C23H36NO11, is orthorhombic, P2(1)2(1)2(1), with Z4, a 6.207(1), b 14.219(1), and c 30.986(2) A. It was solved by use of the MULTAN program and refined to a RW value 0.044, for 2874 observed reflections. It has a head to tail arrangement, each piperidine heterocycle being located between the carbohydrate residues of each neighboring molecule.
Cinget
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Département de Recherche Fondamentale, (U.A.C.N.R.S. 1194), Grenoble, France.
Gagnaire
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Grand
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Vottero
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PJ
D003461:Crystallography; D003497:Cyclic N-Oxides / Q000737:chemistry*; D005947:Glucose / Q000031:analogs & derivatives* / Q000737:chemistry; D008958:Models, Molecular; D013113:Spin Labels
D003497:Cyclic N-Oxides; D013113:Spin Labels; D005947:Glucose; C003959:TEMPO