[Mycotoxins in enzyme preparations. Part II. Method of detection and determination of sterigmatocystin].
A simple method for the detection and semiquantitative determination of sterigmatocystin in enzyme preparations was described. The method comprises extraction with acetonitrile and a 4% aqueous KCL solution, column chromatographic purification of the crude extracts on silica gel, and two-dimensional thin-layer chromatography. The mean recovery by this method is from 71 to 79%, and the detectability of sterigmatocystin is 20 micrograms/kg.
Czerwiecki
L
L
Zakładu Analizy Zywności Instytutu Biotechnologii Przemysłu Rolno-Spozywczego.
D000097:Acetonitriles / Q000737:chemistry; D002855:Chromatography, Thin Layer; D002523:Edible Grain / Q000737:chemistry*; D005504:Food Analysis / Q000379:methods*; D009183:Mycotoxins / Q000032:analysis*; D011189:Potassium Chloride / Q000737:chemistry; D013241:Sterigmatocystin / Q000032:analysis*
D000097:Acetonitriles; D009183:Mycotoxins; D013241:Sterigmatocystin; D011189:Potassium Chloride; C032159:acetonitrile
Mikotoksyny w preparatach enzymatycznych. Cz. II. Metoda wykrywania i oznaczania sterygmatocystyny.