Phase determination by polarized dispersion in vanadyl sulfate pentahydrate.
Anomalous-scattering tensors for V measured with linearly polarized synchrotron radiation in VOSO4. 5H2O near the K-absorption edge exhibit anisotropy as much as 4 units in f" and +/- 2 units in f'. This polarized dispersion causes the diffraction intensity to change when a crystal is turned around a diffraction vector and is the basis of a new way to obtain phases of structure factors.
Templeton
D H
DH
Department of Chemistry, University of California, Berkeley 94720.
Templeton
L K
LK
D008956:Models, Chemical; D015394:Molecular Structure; D011048:Polarography; D012542:Scattering, Radiation; D014639:Vanadium / Q000737:chemistry*; D017968:Vanadium Compounds; D014961:X-Ray Diffraction
D017968:Vanadium Compounds; D014639:Vanadium; C034028:vanadyl sulfate