[The gas chromatographic determination of carbophos in cadaveric material].
The authors developed a method of malathion insecticide determination in the cadaveric material (blood and wall of the stomach) including extraction of 5 ml of blood (5 g of fragmented tissue of stomach wall) by hexan; preparative chromatographic purification of extract on silicagel layer L 5/40 mkm in hexan-diethyl ether system 10:2; Gas-liquid chromatographic investigation on column with 5% SE-30 and 5% XE-60 (Chromatograph "Colour-106" with thermionic detector). This method makes it possible to detect 72-76% of malathion added.
Smirnov
V M
VM
Gorbacheva
N A
NA
D002102:Cadaver; D002849:Chromatography, Gas / Q000295:instrumentation / Q000379:methods*; D006586:Hexanes; D006801:Humans; D008294:Malathion / Q000032:analysis* / Q000302:isolation & purification / Q000506:poisoning; D012997:Solvents; D013270:Stomach / Q000737:chemistry*
D006586:Hexanes; D012997:Solvents; D008294:Malathion
Gazokhromatogreaficheskoe opredelenie karbofosa v trupnom materiale.