[A method of atomic absorption spectrophotometry (AAS) for analysis of cadmium and lead levels in the plant material].
The conditions were evolved and checked for simultaneous determination of cadmium and lead levels in plant material using the flame technique of ASA. For decomposition of the organic substances in plant material wet mineralization was used with a mixture of nitric acid, perchloric acid and sulpuric acid in volume proportions 6:2:0.25. The levels of cadmium and lead were determined in the organic phase after extraction with n-butyl acetate of the previously produced complexes with NaDDTK. The obtained limits of cadmium and lead detectability were 0.002 and 0.02 mg/kg respectively. The recovery rate of the method ranged from 96 to 98%, while the variability index was from 2.6 to 10.2%. The correctness of the evolved analytical procedure was confirmed by determination of the content of both elements in the NBS-SRM 1571 standard (orchard leaves) and by participation in the international interlaboratory investigation of the Polish standard (dried cabbage leaves).
Jedrzejczak
R
R
Zakładu Analizy Zywności Instytutu Biotechnologii Przemysłu Rolno-Spozywczego w Warszawie.
Szteke
B
B
D002104:Cadmium / Q000032:analysis*; D005506:Food Contamination / Q000032:analysis*; D007854:Lead / Q000032:analysis*; D013054:Spectrophotometry, Atomic / Q000379:methods; D014675:Vegetables / Q000032:analysis*
D002104:Cadmium; D007854:Lead
Metoda absorpcyjnej spektrometrii atomowej (ASA) oznaczania zawartości kadmu i ołowiu w materiale roślinnym.