[The analysis of polycyclics in vegetable samples].
PAH analyses in vegetables are often difficult to carry out; therefore two different clean-up methods, which allow elimination of interfering matrix components such as essential oils, waxes, carotinoids and chlorophylls were developed. Clean-up of 32 different vegetables samples consisted of either Bio-Beads S-X3 chromatography or semi-preparative HPLC on silica gel Si-60. PAH were determined by capillary GC-MS, which allowed the application of deuterium-labeled internal standards. The results are presented; higher PAH contamination was detected in kale and parsley.
Speer
K
K
Hygienisches Institut, Chemische und Lebensmitteluntersuchungsanstalt, Hamburg, Bundesrepublik Deutschland.
Horstmann
P
P
Steeg
E
E
Kühn
T
T
Montag
A
A
D002850:Chromatography, Gel; D002851:Chromatography, High Pressure Liquid; D005504:Food Analysis; D008401:Gas Chromatography-Mass Spectrometry; D011083:Polycyclic Compounds / Q000032:analysis*; D014675:Vegetables
D011083:Polycyclic Compounds
Zur Analytik von Polycyclen in Gemüseproben.