Quantitative determination of aluminium in tea by means of aluminium-27 nuclear magnetic resonance spectroscopy.
A method for determining the Al levels in tea leaf digests and tea infusions by means of 27Al nuclear magnetic resonance (NMR) spectroscopy is described. Quantitative results down to 2.0 micrograms cm-3 of Al in 0.5-cm-3 acidified samples are readily obtainable in standard 5-mm NMR tubes. An acceptable quantitative determination is achieved by using an internal Al standard in a 1-mm capillary in conjunction with europium nitrate as a shift reagent.
Koch
K R
KR
Department of Chemistry, University of Cape Town, Rondebosch, Republic of South Africa.
D000535:Aluminum / Q000032:analysis*; D009682:Magnetic Resonance Spectroscopy; D011868:Radioisotopes; D013662:Tea / Q000032:analysis*
D011868:Radioisotopes; D013662:Tea; D000535:Aluminum