Microstructure and mechanical properties of Ti-Ta/alumina and Ti-Nb/alumina joints for dental implants.
The microstructure of Ti-Ta and Ti-Nb alloys diffusion bonded to a 99.7 wt% Al2O3 ceremic for dental implants is subdivided into a reaction double layer containing the phases TiAl and Ti3Al, a transition region of coarse alpha-Ti plates in beta-Ti, and the unaffected bulk metal, the alpha-Ti/beta-Ti structure of which can be refined by annealing at 800 degrees C for 1 hour after bonding. Optimized joints fabricated by diffusion bonding in a high vacuum at 1,200 degrees C from a 99.7 wt% Al2O3 ceramic and Ti-Ta alloys fitted in their thermal contraction behavior to that of the ceramic by the addition of 30 to 40 wt% Ta showed a fracture resistance of 2.3 MN/m3/2. Approximately 80% of the bend test specimens notched at the Ti-Ta/alumina interface failed by crack extension parallel to the interface within the ceramic, which is typical for a metal-ceramic bond of high to medium interfacial strength.
Gibbesch
B
B
Elssner
G
G
Petzow
G
G
D000537:Aluminum Oxide; D003722:Dental Alloys; D001840:Dental Bonding; D003758:Dental Implantation, Endosseous / Q000295:instrumentation*; D015921:Dental Implants; D009556:Niobium; D013635:Tantalum; D014025:Titanium
D003722:Dental Alloys; D015921:Dental Implants; D009556:Niobium; D013635:Tantalum; D014025:Titanium; D000537:Aluminum Oxide