title: [The structure determination of a new alkaloid phlegmariuine-N by long-range two-dimensional and NOE difference NMR spectroscopy].
abstract: A new alkaloid, phlegmariuine-N, was isolated from Phlegmariurus fordii (Baker) Ching. In the present work, a technique of long-range 1H-1H and 13C-1H COSY in combination with NOE difference spectroscopy has been successfully used to connect the spin systems separated by quatermary carbons and heteroatom. Its structure has been elucidated as (I).
authors: Z C
authors: ZC
authors: Miao
authors: Z S
authors: ZS
authors: Yang
authors: R
authors: R
authors: Feng
mesh_terms: D000470:Alkaloids / Q000302:isolation & purification*; D055598:Chemical Phenomena; D002621:Chemistry; D009682:Magnetic Resonance Spectroscopy / Q000379:methods; D014197:Trees
chemical_list: D000470:Alkaloids; C061426:phlegmariuine N