Measurement of plasma oxalate by capillary gas chromatography and its validation by isotope dilution mass spectrometry.
A capillary gas chromatographic method for plasma oxalate and an isotope dilution mass spectrometric reference method, both using the same tert.-butyldimethylsilyl derivatives, are described. Similar reference ranges for both were found (4.93 +/- 1.48 and 4.70 +/- 1.44 mumol/l, respectively), together with a close correlation for results covering a wide range of oxalate concentrations.
France
N C
NC
Department of Pathology, Waikato Hospital, Hamilton, New Zealand.
Holland
P T
PT
McGhie
T K
TK
Wallace
M R
MR
D002250:Carbon Radioisotopes; D002849:Chromatography, Gas; D006801:Humans; D007201:Indicator Dilution Techniques; D007202:Indicators and Reagents; D013058:Mass Spectrometry; D017646:Organosilicon Compounds; D010070:Oxalates / Q000097:blood*; D012825:Silicon
D002250:Carbon Radioisotopes; D007202:Indicators and Reagents; D017646:Organosilicon Compounds; D010070:Oxalates; C009660:t-butyldimethylsilyl compounds; D012825:Silicon