Gas and liquid chromatography of hydroxybiphenyls, chlorinated hydroxybiphenyls and several types of halogenated derivatives. I. Capillary gas chromatography and mass spectrometry.
For 8 hydroxybiphenyls and 19 chlorinated hydroxybiphenyls derivatization reactions with 6 electrophilic reagents--viz., 4 perfluoro anhydrides, pentafluorobenzoyl chloride and tert.-butylpentafluorophenylmethylchlorosilane--have been studied to evaluate their potential for capillary gas chromatography with electron-capture detection. For some of the classes of derivatives, mass spectrometric data are presented.
D001713:Biphenyl Compounds / Q000032:analysis*; D008401:Gas Chromatography-Mass Spectrometry; D011078:Polychlorinated Biphenyls / Q000032:analysis*
D001713:Biphenyl Compounds; D011078:Polychlorinated Biphenyls