Chemical protective clothing standard test method development: Part II. Degradation test method.
A "round-robin" interlaboratory evaluation of a proposed American Society for Testing and Materials (ASTM) standard test method was conducted for measuring the resistance of chemical protective clothing materials to degradation by liquid chemicals. The objective of this project was to determine the relative precision of the method and, where appropriate, recommend modifications that would improve reliability. In the round-robin format, eight laboratories used the proposed method to test each of five protective clothing materials against five liquid chemicals that are widely used commercially. The resulting data revealed that the proposed test method was not stringent enough to generate acceptable levels of accuracy and precision. Both intra- and interlaboratory standard deviations showed a high degree of variability in changes for the three physical properties evaluated. Changes in the method were identified which, if implemented, should improve accuracy and precision considerably.
Coletta
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Tillinghast, a Towers Perrin Company, San Francisco, CA 94104.
Mansdorf
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Berardinelli
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SP
D002074:Butanones; D055598:Chemical Phenomena; D002627:Chemistry, Physical; D006256:Hazardous Waste; D006586:Hexanes; D006801:Humans; D006851:Hydrochloric Acid; D011481:Protective Clothing / Q000592:standards*; D012997:Solvents; D014050:Toluene; D014867:Water
D002074:Butanones; D006256:Hazardous Waste; D006586:Hexanes; D012997:Solvents; D014867:Water; D014050:Toluene; C005222:methylethyl ketone; D006851:Hydrochloric Acid