Rapid method for the detection and quantification of N-nitrosodibutylamine in rubber products.
A rapid method for the detection and quantification of N-nitrosodibutylamine (NDBA) migrating from rubber products into a neutral buffer solution is described. The extraction, clean up, and concentration is done by a one-step procedure using C18 cartridges. NDBA in the ppb range is identified and quantitated by gas chromatography (GC) with a thermal energy analyzer (TEA) as detector.
Zwickenpflug
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W
Walther-Straub-Institut für Pharmakologie und Toxikologie, Ludwig-Maximilians-Universität München, Federal Republic of Germany.
Richter
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E
D002849:Chromatography, Gas; D009602:Nitrosamines / Q000032:analysis*; D012408:Rubber / Q000032:analysis*
D009602:Nitrosamines; C012279:dibutylnitrosamine; D012408:Rubber