Extraction of light filth from rice flours, extruded rice products, and rice paper: collaborative study.
Two new methods were developed for the extraction of rodent hairs and insect fragments from rice products: one for rice flour and one for extruded rice products and rice paper. A 100 g sample of rice flour was extracted with mineral oil-40% isopropanol, followed by a water phase as needed for additional cycles. For extruded rice products and rice paper, a 225 g sample of each was initially extracted as above, followed by a single extraction with mineral oil-20% isopropanol. Both methods used an acid hydrolysis pretreatment followed by wet sieving and a percolator extraction. Average rodent hair recoveries were 77.8% for rice flour and 82.2% for extruded rice products and rice paper. Average insect fragment recoveries were 89.6% for rice flour and 91.9% for extruded rice products and rice paper. Both methods were adopted official first action.
D000818:Animals; D005433:Flour / Q000032:analysis*; D005506:Food Contamination / Q000032:analysis*; D006197:Hair; D007313:Insecta; D012275:Oryza / Q000032:analysis*; D012377:Rodentia