[Synthesis of glycosides. Direct high-performance liquid chromatographic determination of intermediate perbenzylated anomers (author's transl)].
High-performance liquid chromatography has been used to determine the stereospecificity of the synthesis of alpha or beta glycosides. The protecting groups are benzylic ethers, therefore we have employed reversed-phase liquid chromatography to separate alpha and beta anomers. Some octadecyl supports have been compared, in order to optimize the separation for several glycosides.
D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D006027:Glycosides / Q000032:analysis*; D013237:Stereoisomerism
D006027:Glycosides
Dosage direct des anomères perbenzylés intermédiaires par chromatographie en phase liquide à haute performance.