Microcolumn chromatographic cleanup and GLC determination of 11-methyl-16,16-dimethylprostaglandin E2 in polyethylene glycol 400 solutions.
An analytical procedure is described for the GLC determination of 11-methyl-16,16-dimethylprostaglandin E2 in aqueous polyethylene glycol 400 solutions. Because of the nature of the carrier matrix, sample cleanup was required prior to GLC separation. Separation was achieved using a diethylaminoethylcellulose microcolumn. This procedure has proven to be amenable to routine analysis.
D015064:16,16-Dimethylprostaglandin E2 / Q000031:analogs & derivatives / Q000032:analysis*; D002849:Chromatography, Gas; D008722:Methods; D011092:Polyethylene Glycols; D011459:Prostaglandins E, Synthetic / Q000032:analysis*
C027057:11-methyl-16,16-dimethylprostaglandin E2; D011459:Prostaglandins E, Synthetic; D011092:Polyethylene Glycols; D015064:16,16-Dimethylprostaglandin E2