A simple procedure for extracting methacrylic acid from water-miscible methacrylates.
A simple procedure for removing methacrylic acid from water-miscible methacrylates is described. One volume of monomer is diluted with 9 volumes of diethyl ether. Three consecutive extractions are carried out with 5% aqueous NaHCO3 at 4 C. Residual water is removed by shaking with anhydrous sodium sulfate. The ether is removed by flash evaporation on a Büchi Rotavapor. Weak alkali extraction produces good quality semithin sections which are free of background staining. This method may be a useful alternative to existing methods for removal of methacrylic acid.
D000179:Acrylates / Q000032:analysis* / Q000302:isolation & purification*; D008689:Methacrylates / Q000032:analysis* / Q000302:isolation & purification*; D008722:Methods
D000179:Acrylates; D008689:Methacrylates; C008384:methacrylic acid; C005044:hydroxyethyl methacrylate; C032802:hydroxypropyl methacrylate