Mass spectral identification and gas-liquid chromatographic determination of methyl 4-chloroindolyl-3-acetate in canned and frozen peas.
Methyl 4-chloroindolyl-3-acetate (MCIA), a naturally occurring auxin, has been identified in canned and frozen peas by gas-liquid chromatography (GLC)/mass spectrometry. Eight samples were analyzed for MCIA using slightly modified official AOAC multiple pesticide residue procedures employing GLC with microcoulometric detection. Levels of MCIA averaged 0.20 ppm for canned peas and 0.16 ppm for frozen peas. Recovery of MCIA from a fortified sample was 40%.
D002849:Chromatography, Gas; D007887:Fabaceae / Q000032:analysis*; D005519:Food Preservation; D008401:Gas Chromatography-Mass Spectrometry / Q000379:methods; D007210:Indoleacetic Acids / Q000032:analysis*; D010937:Plant Growth Regulators / Q000032:analysis*; D010946:Plants, Medicinal
D007210:Indoleacetic Acids; D010937:Plant Growth Regulators; C028267:methyl 4-chloroindolyl-3-acetate