Data verification in the residue laboratory.
Residue analysis frequently presents a challenge to the quality assurance (QA) auditor due to the sheer volume of data to be audited. In the face of multiple boxes of raw data, some process must be defined that assures the scientist and the QA auditor of the quality and integrity of the data. A program that ensures that complete and appropriate verification of data before it reaches the Quality Assurance Unit (QAU) is presented. The "Guidelines for Peer Review of Data" were formulated by the Residue Analysis Business Center at Ricerca, Inc. to accommodate efficient use of review time and to define any uncertainties concerning what are acceptable data. The core of this program centers around five elements: Study initiation (definitional) meetings, calculations, verification, approval, and the use of a verification checklist.
Ault
J A
JA
Ricerca, Inc., Painesville, Ohio 44077, USA.
Cassidy
P S
PS
Crawford
C J
CJ
Jablonski
J E
JE
Kenyon
R G
RG
D002623:Chemistry Techniques, Analytical / Q000592:standards*; D003627:Data Interpretation, Statistical; D004282:Documentation / Q000379:methods*; D017408:Guidelines as Topic; D007324:Institutional Management Teams; D007753:Laboratories / Q000592:standards*; D017712:Peer Review, Research; D011785:Quality Assurance, Health Care