[The determination of ferroceron in the practice of forensic chemical expertise].
Valov's method followed by extraction of the acid form of ferroceron with ether is recommended for isolation of ferroceron from cadaveric material in forensic chemical practice expert evaluation. Detection and measurement of isolated ferroceron are carried out by thin-layer chromatography and spectroscopy in the visible part of the spectrum. The developed method for ferroceron detection in cadaveric material was used in two expert evaluations. Recommendations are offered on the detection of ferroceron in cadaveric and biological material and on resuscitation measures in cases with poisoning with this drug.
Il'ina
I V
IV
Solomatin
E M
EM
D002102:Cadaver; D002855:Chromatography, Thin Layer / Q000379:methods; D005260:Female; D005296:Ferrous Compounds / Q000032:analysis* / Q000302:isolation & purification / Q000506:poisoning; D005554:Forensic Medicine / Q000379:methods*; D006801:Humans; D007223:Infant; D008099:Liver / Q000737:chemistry; D008297:Male; D009942:Organometallic Compounds / Q000032:analysis* / Q000302:isolation & purification / Q000506:poisoning; D011041:Poisoning / Q000175:diagnosis; D013056:Spectrophotometry, Ultraviolet / Q000379:methods
D005296:Ferrous Compounds; D009942:Organometallic Compounds; C014555:ferroceron
Opredelenie ferrotserona v sudebno-khimicheskoĭ ékspertnoĭ praktike.