Effects of treatment and storage conditions on ceramic/composite bond strength.
During the past few years, the interest in using ceramic inlays and veneers has increased. New materials and methods have been introduced to bond these restorations to resinous materials. Since our knowledge of how to optimize such bonding is limited, the objective of this study was to test the hypothesis that various surface treatment variables and combinations of these variables affect the strength of the ceramic/composite interphase of ceramic inlays differently. The influences of material composition, surface-roughening method, silane treatment, silane heat treatment, and storage condition on bond strength were investigated. Three ceramics (Dicor, Mirage, Vitabloc), three surface-roughening methods (etching, sandblasting, grinding), three silane treatments (gamma-methacryloxypropyltrimethoxysilane [MPS], MPS+paratoluidine, vinyltrichlorosilane), two heat treatments (20 degrees C for 60 s, 100 degrees C for 60 s), and two storage conditions (24-hour dry, one yr in water at 37 degrees C) were studied. For each of the 108 combinations, five specimens were tested. Ceramic cylinders were treated according to group assignment and bonded to blocks of the same ceramic material with a dual-cured resin. The shear bond strength was determined, and the experimental factors were evaluated by analysis of variance. The results showed that surface-roughening method had the strongest effect on bond strength, while ceramic selection had the least significant effect. Of the surface-roughening methods, etching was associated with higher bond strength values than either sandblasting or grinding.(ABSTRACT TRUNCATED AT 250 WORDS)
Roulet
J F
JF
Department of Operative Dentistry and Endodontics North, Freie Universität Berlin, Germany.
Söderholm
K J
KJ
Longmate
J
J
D000537:Aluminum Oxide; D064751:Ammonium Compounds; D000704:Analysis of Variance; D002516:Ceramics / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry*; D001840:Dental Bonding; D003738:Dental Cements / Q000737:chemistry*; D003776:Dental Porcelain / Q000737:chemistry*; D004356:Drug Storage; D005459:Fluorides; D006358:Hot Temperature; D006858:Hydrofluoric Acid; D008422:Materials Testing; D000644:Quaternary Ammonium Compounds; D012821:Silanes / Q000737:chemistry; D013499:Surface Properties; D013718:Tensile Strength
D064751:Ammonium Compounds; D003188:Composite Resins; D003738:Dental Cements; C047475:Dicor ceramic; C080875:Mirage; D000644:Quaternary Ammonium Compounds; D012821:Silanes; D003776:Dental Porcelain; C074543:Cerec; C024822:ammonium fluoride; D000537:Aluminum Oxide; D005459:Fluorides; D006858:Hydrofluoric Acid