title: [Studies on the identification of psychotropic substances. IX. Preparation and various analytical data of reference standard of new psychotropic substances, N-ethyl methylenedioxyamphetamine, N-hydroxy methylenedioxyamphetamine, mecloqualone, 4-methylaminorex, phendimetrazine and phenmetrazine].
abstract: The reference standards of N-Ethyl methylenedioxyamphetamine, N-Hydroxy methylenedioxy-amphetamine, Mecloqualone, 4-Methylaminorex. Phendimetrazine and Phenmetrazine were chemically prepared from commercial chemicals. Their purities determined by HPLC were more than 99.8%. The standard spectra and chromatograms of the standards such as TLC, UV, IR, HPLC, GC/MS and NMR were measured. For the identification of these six drugs in forensic laboratory, their mass fragmentation and NMR spectra were discussed.
authors.forename: M
authors.initials: M
authors.lastname: Shimamine
authors.forename: K
authors.initials: K
authors.lastname: Takahashi
authors.forename: Y
authors.initials: Y
authors.lastname: Nakahara
mesh_terms: D015104:3,4-Methylenedioxyamphetamine / Q000031:analogs & derivatives / Q000592:standards; D002851:Chromatography, High Pressure Liquid; D002855:Chromatography, Thin Layer; D008401:Gas Chromatography-Mass Spectrometry; D009025:Morpholines / Q000592:standards; D010080:Oxazoles / Q000592:standards; D010633:Phenmetrazine / Q000592:standards; D011619:Psychotropic Drugs / Q000302:isolation & purification* / Q000592:standards*; D011799:Quinazolines / Q000592:standards; D013053:Spectrophotometry
chemical_list: D009025:Morpholines; D010080:Oxazoles; D011619:Psychotropic Drugs; D011799:Quinazolines; C100281:mecloqualone; D015104:3,4-Methylenedioxyamphetamine; C062690:N-hydroxy-1-(3,4-methylenedioxyphenyl)-2-aminopropane; C000081:4-methylaminorex; C100294:phendimetrazine; C051800:3,4-methylenedioxyethamphetamine; D010633:Phenmetrazine