[Determination of major volatile components in suhexiang wan (storax pill) using analytical supercritical fluid extraction (SFE)].
A new method based on the off-line coupling of analytical SFE and GC has been developed for qualitative and quantitative analysis of major volatile components in Suhexiang Wan, a Chinese patent medicine. The factors affecting extraction efficiency were examined to seek the optimal operating parameters. Quantitative recovery (90%) was achieved with 20 ml CO2 in ca 1 h using a self-designed analytical SFE system. Compared with the conventional methods, the SFE as an alternative technique for sample preparation will be most useful in the quality control of Chinese patent medicine.
Ma
X Z
XZ
Department of Applied Chemistry, Beijing Institute of Chemical Technology.
Yu
X B
XB
Chen
J J
JJ
Liang
Z M
ZM
Coa
T C
TC
Wang
Y
Y
D001565:Benzoates; D001892:Camphanes / Q000032:analysis; D003516:Cycloparaffins; D004338:Drug Combinations; D004365:Drugs, Chinese Herbal / Q000737:chemistry*; D005054:Eugenol / Q000032:analysis
D001565:Benzoates; D001892:Camphanes; D003516:Cycloparaffins; D004338:Drug Combinations; D004365:Drugs, Chinese Herbal; D005054:Eugenol; C022871:isoborneol; C006723:benzyl benzoate; C031021:muscone