Determination of cymiazole residues in honey by liquid chromatography.
A liquid chromatographic method is described for the determination of cymiazole residues in honey. This acaricide is determined on a reversed-phase (C18) column, with a CH3CN-0.001N HCl-NaCl mixture (950 mL + 50 mL + 0.3 g/L) as the mobile phase, and UV detection at 265 nm. Cymiazole is extracted with n-hexane from aqueous alkalinized (pH 9) honey solutions. No further cleanup of the honey extract was required before chromatographic analysis. Recoveries on control samples fortified with 0.01, 0.10, and 1.00 ppm cymiazole ranged from 92 to 102%. The limit of determination was 0.01 ppm.
Cabras
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Dipartimento di Tossicologia, Cagliari, Italy.
Melis
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Spanedda
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D002853:Chromatography, Liquid; D005506:Food Contamination; D006722:Honey / Q000032:analysis*; D010573:Pesticide Residues / Q000032:analysis*; D013844:Thiazoles / Q000032:analysis*
D010573:Pesticide Residues; D013844:Thiazoles; C080031:cymiazole