2H-->1H cross-polarization in deuterated glycine.
1H spectral details and CP kinetics are discussed. We recommend perdeuterated polycrystalline glycine as a standard for setting 2H-->1H cross-polarization (CP), for 1H chemical shift referencing and for checking the setting of the magic angle and the shims.
Kolodziejski
W
W
Instituto de Technología Quimica UPV-CSIC, Universidad Politécnica de Valencia, Spain.
Corma
A
A
D003903:Deuterium / Q000737:chemistry*; D005998:Glycine / Q000737:chemistry*; D007700:Kinetics; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D008968:Molecular Conformation; D011522:Protons
D011522:Protons; D003903:Deuterium; D005998:Glycine