title: [The analysis of grandaksin in cadaveric material].
abstract: Grandaxine was measured in expert cadaveric material (gastric wall, small intestine, and kidney) by thin layer and liquid chromatography and UV spectroscopy. Chromatographic measurement in a thin layer of the adsorbent was carried out on L 5/40 M plates in the following solvent systems: tholuene-acetone-25% ammonium hydroxide (50:50:1); ethyl acetate-methanol-25% ammonium hydroxide (17:2:1); chloroform-methanol (9:1); and chloroform-acetone (9:1). Analysis by high-pressure liquid chromatography was carried out by means of a Milichrome-4 chromatographer with a UV detector on the column packed with Separone C18 (5 mcm) using a mobile phase acetonitrile-0.05 M disubstituted ammonium phosphate (55:45).
authors.forename: D E
authors.initials: DE
authors.lastname: Bodrina
authors.forename: V S
authors.initials: VS
authors.lastname: Galkina
authors.forename: S K
authors.initials: SK
authors.lastname: Eremin
authors.forename: E M
authors.initials: EM
authors.lastname: Salomatin
mesh_terms: D014151:Anti-Anxiety Agents / Q000032:analysis*; D000928:Antidepressive Agents / Q000032:analysis*; D001569:Benzodiazepines / Q000032:analysis*; D002102:Cadaver; D002851:Chromatography, High Pressure Liquid / Q000379:methods / Q000706:statistics & numerical data; D002855:Chromatography, Thin Layer / Q000379:methods / Q000706:statistics & numerical data; D006801:Humans; D007421:Intestine, Small / Q000737:chemistry*; D007668:Kidney / Q000737:chemistry*; D013056:Spectrophotometry, Ultraviolet; D013270:Stomach / Q000737:chemistry*; D013607:Tablets
chemical_list: D014151:Anti-Anxiety Agents; D000928:Antidepressive Agents; D013607:Tablets; D001569:Benzodiazepines; C012582:tofisopam