Determining temperature in a magic-angle spinning probe using the temperature dependence of the isotropic chemical shift of lead nitrate.
The calibration of temperature in a magic-angle spinning probe with lead nitrate is discussed. The effects of rotation frequency on temperature are demonstrated.
Neue
G
G
University of Dortmund, Germany.
Dybowski
C
C
D007854:Lead; D009682:Magnetic Resonance Spectroscopy; D009566:Nitrates; D012399:Rotation; D013696:Temperature
D009566:Nitrates; D007854:Lead; C017461:lead nitrate