title: High resolution and high fields in biological solid state NMR.
abstract: 2H solid state NMR spectra of a polypeptide in an oriented membrane environment is demonstrated to have an orientational resolution of 0.3 degree. Such data results in high resolution structural constraints. Similar spectra are demonstrated at 23.2 T using a resistive magnet at the National High Magnetic Field Laboratory.
authors.affiliation: National High Magnetic Field Laboratory, Institute for Molecular Biophysics, Florida State University, Tallahassee 32306-4005, USA.
authors.forename: M
authors.initials: M
authors.lastname: Cotten
authors.forename: V G
authors.initials: VG
authors.lastname: Soghomonian
authors.forename: W
authors.initials: W
authors.lastname: Hu
authors.forename: T A
authors.initials: TA
authors.lastname: Cross
mesh_terms: D000900:Anti-Bacterial Agents / Q000737:chemistry; D006096:Gramicidin / Q000737:chemistry; D006801:Humans; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000295:instrumentation
chemical_list: D000900:Anti-Bacterial Agents; D006096:Gramicidin