High resolution and high fields in biological solid state NMR.
2H solid state NMR spectra of a polypeptide in an oriented membrane environment is demonstrated to have an orientational resolution of 0.3 degree. Such data results in high resolution structural constraints. Similar spectra are demonstrated at 23.2 T using a resistive magnet at the National High Magnetic Field Laboratory.
Cotten
M
M
National High Magnetic Field Laboratory, Institute for Molecular Biophysics, Florida State University, Tallahassee 32306-4005, USA.
Soghomonian
V G
VG
Hu
W
W
Cross
T A
TA
D000900:Anti-Bacterial Agents / Q000737:chemistry; D006096:Gramicidin / Q000737:chemistry; D006801:Humans; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000295:instrumentation
D000900:Anti-Bacterial Agents; D006096:Gramicidin