Structure and fluorometric HPLC determination of 1-desulfoyessotoxin, a new yessotoxin analog isolated from mussels from Norway.
A new analog of yessotoxin, 1-desulfoyessotoxin, was isolated from the digestive glands of mussels growing in the Sognefjord, Norway. Its structure was determined by NMR and negative ion CID MS/MS experiments. 1-Desulfoyessotoxin can be detected by the fluorometric HPLC method analogous with other yessotoxins.
Daiguji
M
M
Department of Applied Bioorganic Chemistry, Graduate School of Agricultural Science, Tohoku University, Tsutsumidori-Amamiya, Aoba-ku, Sendai, Japan.
Satake
M
M
Ramstad
H
H
Aune
T
T
Naoki
H
H
Yasumoto
T
T
D000818:Animals; D049872:Bivalvia / Q000737:chemistry*; D002851:Chromatography, High Pressure Liquid; D004988:Ethers, Cyclic / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D008978:Mollusk Venoms / Q000737:chemistry*; D009664:Norway; D013050:Spectrometry, Fluorescence; D016339:Spectrometry, Mass, Fast Atom Bombardment
C401106:1-desulfoyessotoxin; D004988:Ethers, Cyclic; D008978:Mollusk Venoms