Various applications of liquid chromatography-mass spectrometry to the analysis of phenolic compounds.
Different options of liquid chromatography-mass spectrometry were used to establish the most suitable ion source and conditions to analyse or detect some low-molecular mass phenols, flavan-3-ols, and apply such conditions to a complex sample (wine). Data presented in this work confirm the great utility of atmospheric pressure-ionisation electrospray mass spectrometry coupled to HPLC for analysis of phenolic compounds, under negative mode in the case of low-molecular mass phenols, and under both positive and negative modes in flavan-3-ol compounds. A fragmentor voltage of 60 V could be the most suitable for analysing the compounds under study.
Pérez-Magariño
S
S
Department of Biotechnology and Food Science, University of Burgos, Spain.
Revilla
I
I
González-SanJosé
M L
ML
Beltrán
S
S
D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D013058:Mass Spectrometry / Q000379:methods*; D010636:Phenols / Q000032:analysis*; D014920:Wine / Q000032:analysis*
D010636:Phenols