Stable Polymer-Bound Iodine Azide.
1,2-Azido-iodination of a wide range of alkenes under very mild conditions can be achieved by using a novel iodate(I) reagent, a stable and storable polymer-bound iodine azide, which is available in two steps (see scheme). Simple work-up and convenient use in automated parallel synthesis are important features of this polymer-bound reagent.
Kirschning
A
Institut für Organische Chemie der Technische Universität Clausthal, Leibnizstrasse 6, D-38678 Clausthal-Zellerfeld (Germany).
Monenschein
H
Schmeck
C