Combinatorial Methods for the Synthesis of Aluminophosphate Molecular Sieves.
Automatic dispensing of reagents into autoclave blocks followed by synthesis, isolation, and automated structure analysis with X-ray diffractometry represents an efficient methodology for the combinatorial synthesis of microporous materials. The figure shows a typical diffractogram of as-synthesized AFI-type molecular sieves taken with a CCD camera.
Choi
K
Department of Chemistry, Purdue University, West Lafayette, IN 47906 (USA).
Gardner
D
Hilbrandt
N
Bein
T