2-Alkylcyclobutanones as markers for irradiated foodstuffs. III. Improvement of the field of application on the EN 1785 method by using silver ion chromatography.
The inclusion of a purification step by silver ion chromatography in the EN 1785 analytical protocol for 2-alkylcyclobutanones (validated by the European Committee for Standardization for the detection of ionizing radiation treatment) has considerably improved the quality of the chromatograms obtained, allowing the detection of food samples irradiated at very low doses (0.1 kGy) or irradiated ingredients included in low proportions in non irradiated foodstuffs. This analytical modification of the protocol EN 1785 ought thus to permit a very considerable extension of its current field of application.
Ndiaye
B
B
Département des Sciences de l'Aliment, Faculté de Pharmacie, Illkirch, France.
Horvatovich
P
P
Miesch
M
M
Hasselmann
C
C
Marchioni
E
E
D002074:Butanones / Q000032:analysis*; D002853:Chromatography, Liquid / Q000379:methods*; D005514:Food Irradiation; D008401:Gas Chromatography-Mass Spectrometry; D011829:Radiation Dosage; D012834:Silver / Q000737:chemistry
D002074:Butanones; D012834:Silver