title: An efficient synthesis of two monosulfated trisaccharides with the Galbeta1,3GlcNacbeta1,3Galbeta-O-allyl backbone.
abstract: The GlcNAcbeta(1-->3) Gal linked disaccharide 7 was synthesized as key building blocks for the construction of target monosulfated trisaccharides 1 and 2 using oxazoline 3 as glycosyl donor promoted by BF3 x Et2O.
authors.affiliation: Department of Molecular & Cellular Biophysics, Roswell Park Cancer Institute, Buffalo, NY 14263, USA.
authors.forename: J
authors.initials: J
authors.lastname: Xia
authors.forename: C F
authors.initials: CF
authors.lastname: Piskorz
authors.forename: R D
authors.initials: RD
authors.lastname: Locke
authors.forename: E V
authors.initials: EV
authors.lastname: Chandrasekaran
authors.forename: J L
authors.initials: JL
authors.lastname: Alderfer
authors.forename: K L
authors.initials: KL
authors.lastname: Matta
mesh_terms: D002240:Carbohydrate Sequence; D009682:Magnetic Resonance Spectroscopy; D008969:Molecular Sequence Data; D009844:Oligosaccharides / Q000138:chemical synthesis* / Q000737:chemistry; D013431:Sulfates / Q000737:chemistry*
chemical_list: D009844:Oligosaccharides; D013431:Sulfates