Analysis of pesticide residues in fruit and vegetables after cleanup with solid-phase extraction using ENV+ (Polystyrene-divinylbenzene) cartridges.
A rapid and simple cleanup procedure for the existing multimethod using solid-phase extraction columns to measure pesticide concentrations in fruit and vegetables is presented. After extraction with ethyl acetate, the sample is passed through ENV+, polystyrene-divinylbenzene extraction column, and eluted with ethyl acetate and injected on to capillary GC columns connected to various detectors. The extraction column has the capacity to retain a broad range of pesticides and is widely used in environmental water samples. In this paper, the sample is extracted in an organic solvent. In contrast to what could be expected, it has been found that the column has the capacity to retain pesticides when used as the normal phase.
Pihlström
T
T
National Food Administration, P.O. Box 622, S-751 26 Uppsala, Sweden.
Osterdahl
B G
BG
D002849:Chromatography, Gas; D002853:Chromatography, Liquid / Q000379:methods*; D005638:Fruit / Q000737:chemistry*; D010573:Pesticide Residues / Q000032:analysis* / Q000302:isolation & purification; D011137:Polystyrenes / Q000737:chemistry; D020058:Styrene / Q000737:chemistry; D014675:Vegetables / Q000737:chemistry*
D010573:Pesticide Residues; D011137:Polystyrenes; D020058:Styrene