207Pb chemical shift thermometer at high temperature for magic angle spinning experiments.
The temperature dependence of 207Pb chemical shift in magic angle spinning (MAS) NMR spectrum of Pb(NO3)2 provides a sensitive method to calibrate sample temperatures in MAS NMR. The temperature dependence is uniform in the temperature range between 30 degrees C and 400 degrees C. The NMR sensitivity and the line width are also favorable.
Takahashi
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Japan Energy Analytical Research Center, Toda, Saitama, Japan.
Kawashima
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Sugisawa
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Baba
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D006358:Hot Temperature; D007554:Isotopes; D007854:Lead / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D009566:Nitrates / Q000737:chemistry*; D013821:Thermometers
D007554:Isotopes; D009566:Nitrates; D007854:Lead; C017461:lead nitrate