title: 207Pb chemical shift thermometer at high temperature for magic angle spinning experiments.
abstract: The temperature dependence of 207Pb chemical shift in magic angle spinning (MAS) NMR spectrum of Pb(NO3)2 provides a sensitive method to calibrate sample temperatures in MAS NMR. The temperature dependence is uniform in the temperature range between 30 degrees C and 400 degrees C. The NMR sensitivity and the line width are also favorable.
authors.affiliation: Japan Energy Analytical Research Center, Toda, Saitama, Japan.
authors.forename: T
authors.initials: T
authors.lastname: Takahashi
authors.forename: H
authors.initials: H
authors.lastname: Kawashima
authors.forename: H
authors.initials: H
authors.lastname: Sugisawa
authors.forename: T
authors.initials: T
authors.lastname: Baba
mesh_terms: D006358:Hot Temperature; D007554:Isotopes; D007854:Lead / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D009566:Nitrates / Q000737:chemistry*; D013821:Thermometers
chemical_list: D007554:Isotopes; D009566:Nitrates; D007854:Lead; C017461:lead nitrate