The hair analysis proficiency testing program of the French Society of Analytical Toxicology.
In an effort to improve laboratories performing hair analysis in forensic cases, the French Society of Analytical Toxicology (S.F.T.A.) has implemented a proficiency testing program since 1992. Actually about 10 laboratories are participating. Each survey is dedicated to one analyte or one pharmacological class: opiates (6-monoacetylmorphine, morphine and codeine), cocaine and benzoylecgonine, tetrahydrocannabinol, buprenorphine and norbuprenorphine, beta-blockers (metoprolol, atenolol), beta 2-agonists (salbutamol, clenbuterol). Animal hair was tested for clenbuterol. Prior to sending, hair samples were reduced to a powdered form, well mixed to ensure homogeneity, and then tested by GC/MS or HPLC/MS. Results confirm those obtained in a preliminary study on opiates and cocaine analysis in hair: a common analytical procedure has to be used by all the participants, including hydrolysis of hair. It is essential to work on authentic drug-positive hair samples and not on spiked samples. Participation at this program is free of charge and considered as an educational tool. Comparison of the results with those of other laboratories in Europe and USA shows that the analytical methods used during this program are in accordance with all the other procedures.
Deveaux
M
M
Institut de Médecine Légale, Lille, France.
Kintz
P
P
Goullé
J P
JP
Bessard
J
J
Pépin
G
G
Gosset
D
D
D002851:Chromatography, High Pressure Liquid / Q000592:standards; D003042:Cocaine / Q000032:analysis; D005602:France; D008401:Gas Chromatography-Mass Spectrometry / Q000592:standards; D006197:Hair / Q000737:chemistry*; D006801:Humans; D007753:Laboratories / Q000592:standards*; D013058:Mass Spectrometry / Q000592:standards; D009294:Narcotics / Q000032:analysis; D011786:Quality Control; D015813:Substance Abuse Detection / Q000592:standards*; D014116:Toxicology / Q000592:standards
D009294:Narcotics; D003042:Cocaine