[Assay of terpenes in the leaves of Ginkgo biloba extract and its preparations by in situ fluorometric TLC].
A new TLC method for the assay of terpene lactones in Ginkgo biloba extract and its preparations has been established by means of optimized development condition and post-chromatographic thermal fluorescence derivatization. Satisfactory results can be obtained through polynomial regression calibration. The data obtained by this method have been proved ten times higher in sensitivity than those obtained by HPLC-refracto-detector.
Yan
Y
Y
Guangzhou Mumicipal Institute for Drug Control.
Xie
P
P
Qian
H
H
Lin
Q
Q
D002851:Chromatography, High Pressure Liquid / Q000379:methods; D002855:Chromatography, Thin Layer / Q000379:methods; D003517:Cyclopentanes / Q000032:analysis*; D004224:Diterpenes; D004365:Drugs, Chinese Herbal / Q000737:chemistry*; D005663:Furans / Q000032:analysis*; D020441:Ginkgo biloba / Q000737:chemistry*; D046934:Ginkgolides; D007783:Lactones / Q000032:analysis*; D018515:Plant Leaves / Q000737:chemistry; D010946:Plants, Medicinal; D013729:Terpenes / Q000032:analysis
D003517:Cyclopentanes; D004224:Diterpenes; D004365:Drugs, Chinese Herbal; D005663:Furans; D046934:Ginkgolides; D007783:Lactones; D013729:Terpenes; C058295:ginkgolide C; C045856:ginkgolide B; C073710:bilobalide