Effect of cooling condition on leucite crystals in dental porcelains.
X-ray diffractometry (XRD) was used to analyze the crystal phases of three commercial dentin and incisal porcelains prepared by normal cooling, quenching in water, and controlled slow annealing after normal firing. There were no remarkable differences in the contents of either tetragonal and cubic leucite in the fired porcelain discs prepared under the three cooling conditions. Furthermore, there were no significant differences in the parameters of the a-axis and c-axis of tetragonal leucite, and the a-axis of cubic leucite among them. These results suggest that the cooling condition has little effect on the microstructural changes of leucite crystals in the dental porcelains, since the leucite crystals were formed at a higher temperature range than the firing- and cooling-temperature range and were stabilized by incorporation of additives into the lattice.
Ban
S
S
Department of Dental Material Science, Aichi-Gakuin University, Nagoya, Japan.
Matsuo
K
K
Mizutani
N
N
Tanikawa
H
H
Kaikawa
K
K
Hasegawa
J
J
D000538:Aluminum Silicates / Q000737:chemistry*; D003080:Cold Temperature; D018360:Crystallography, X-Ray; D003776:Dental Porcelain / Q000737:chemistry*; D008422:Materials Testing; D015394:Molecular Structure; D008970:Molecular Weight; D013052:Spectrometry, X-Ray Emission
D000538:Aluminum Silicates; D003776:Dental Porcelain; C078519:leucite