Effects of thermal cycling on dynamic viscoelastic properties of four commercial resins for crown and bridge.
To elucidate the effects of thermal cycling on the viscoelastic properties of four commercial resins for crown and bridge, dynamic shear modulus (G'), mechanical loss tangent (tan delta), Knoop hardness, water sorption and appearance of specimen surfaces before and after thermal cycling test were determined. The changes of G' and tan delta for two materials were insignificant with increased repetitions of thermal cycling. Those of the other two materials were statistically significant: in particular, G' at temperatures above 60 degrees C was inclined to increase slightly and tan delta decreased considerably. While the Knoop hardness of the materials was a little decreased over a number of 75,000 thermal cycles, the water sorption almost attained an equilibrium in uptake after 14,000 thermal cycles. Furthermore, cracks on the specimen surface were observed after 37,500 to 75,000 thermal cycles. From these results, the deterioration of materials was observed as damage to the specimen surface. Moreover, it could be presumed that the materials would be further polymerized during the period of thermal cycling.
Fujii
K
K
Department of Biomaterials Science, Kagoshima University Dental School, Japan.
Miura
K
K
Omori
K
K
Arikawa
H
H
Kanie
T
T
Inoue
K
K
D000704:Analysis of Variance; D003188:Composite Resins / Q000737:chemistry*; D003801:Dental Veneers; D004548:Elasticity; D006244:Hardness; D006358:Hot Temperature; D008422:Materials Testing; D011108:Polymers / Q000737:chemistry; D018709:Statistics, Nonparametric; D013499:Surface Properties; D014783:Viscosity; D017155:Wettability
D003188:Composite Resins; D011108:Polymers