Efficient large-scale radical deoxygenation in alcoholic solvents using sodium hypophosphite and a phase-transfer agent: application to erythromycins.
Graham
A E
AE
Process Development, Chemical and Agricultural Products Division, Abbott Laboratories, North Chicago, Illinois 60064-4000, USA.
Thomas
A V
AV
Yang
R
R
D000438:Alcohols; D000900:Anti-Bacterial Agents / Q000737:chemistry*; D018360:Crystallography, X-Ray; D004917:Erythromycin / Q000737:chemistry*; D005609:Free Radicals / Q000737:chemistry; D007202:Indicators and Reagents; D009682:Magnetic Resonance Spectroscopy; D010721:Phosphinic Acids; D012997:Solvents
D000438:Alcohols; D000900:Anti-Bacterial Agents; D005609:Free Radicals; D007202:Indicators and Reagents; D010721:Phosphinic Acids; D012997:Solvents; D004917:Erythromycin; C009287:sodium hypophosphite