Gas chromatography-mass spectrometry-Fourier transform infrared spectrometry and high-performance liquid chromatographic characterization of mononitro- and dinitro-isomers from the nitration of N,N-dimethyldiphenylacetamide.
Gas chromatographic retention data, Fourier transform infrared and mass spectrometric (electron impact, electron attachment and methane chemical ionization) profiles are reported for the products of mono- and dinitration of N,N-dimethyldiphenylacetamide. Differentiations of analytical importance among isomers could be gathered by the study which led to their complete identification.
Soják
L
L
Institute of Chemistry, Faculty of Natural Sciences, Comenius University, Bratislava, Slovak Republic. sojak@fns.uniba.sk
Perjéssy
A
A
Kubinec
R
R
Cambáliková
J
J
Giumanini
A G
AG
Verardo
G
G
Magnan
M M
MM
D000081:Acetamides / Q000032:analysis*; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D008401:Gas Chromatography-Mass Spectrometry / Q000379:methods*; D007536:Isomerism; D017550:Spectroscopy, Fourier Transform Infrared / Q000379:methods*
D000081:Acetamides