Simultaneous determination of beauvericin, enniatins, and fusaproliferin by high performance liquid chromatography.
A rapid, sensitive and inexpensive HPLC method for routine screening of beauvericin, fusaproliferin, and enniatin B(1), A(1), and B has been optimized. Detection limits were determined, ranging between 0. 5 and 3.6 ng according to the compound obtained after spiking samples with each mycotoxin at 10-56 microg/mL concentration range; recoveries averaging from 56 to 74% were obtained. LC-MS conditions for enniatin analyses by API electrospray technique were set up, this allowing a unique identification of three different enniatins.
Monti
S M
SM
Dipartimento di Scienza degli Alimenti, Università degli Studi di Napoli "Federico II", Italy.
Fogliano
V
V
Logrieco
A
A
Ferracane
R
R
Ritieni
A
A
D000900:Anti-Bacterial Agents / Q000032:analysis*; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D047630:Depsipeptides; D010455:Peptides; D012680:Sensitivity and Specificity; D013729:Terpenes / Q000032:analysis*
D000900:Anti-Bacterial Agents; D047630:Depsipeptides; D010455:Peptides; D013729:Terpenes; C100264:enniatins; C093577:fusaproliferin; C004456:beauvericin