Bis
The title double salt, [Ni(C(2)H(8)N(2))(3)](2)(SbS(4))(NO(3)), was crystallized under solvothermal conditions. Hydrogen bonds between the SbS(4)(3-) anions (at four sites) and the [Ni(en)(3)](2+) (en = ethylenediamine) cations (at two sites) form a three-dimensional network. The NO(3)(-) anion is disordered over four sites. The cation lies on a twofold rotation axis and the SbS(4)(3-) anion on a -4 axis.
Schur
M
Institut fur Anorganische Chemie, Christian-Albrechts-Universitat Kiel, Olshausenstrasse 40, D-24089 Kiel, Germany.
Bensch
W