Na2Fe(CN)5(NO).2D2O at 11 and 293 K by X-ray, and at 15 K by neutron diffraction.
The crystal structure of Na(2)Fe(CN)(5)(NO).2D(2)O, disodium pentacyanonitrosylferrate(III) bis(dideuterium oxide), has been determined by X-ray diffraction at 11 and 293 K, and by neutron diffraction at 15 K. The accurate and extensive data sets lead to more precise determinations than are available from earlier work. The agreement in atomic positional and displacement parameters between the determinations at low temperature is very good.
Schultz
A J
AJ
Intense Pulsed Neutron Source, Argonne National Laboratory, Argonne, IL 60439-4814, USA.
Figgis
B N
BN
Sobolev
A N
AN