Simultaneous direct high-performance liquid chromatographic enantioseparation of 2-methylglycidol-1-benzyl ether and 2-methylglycerol-1-benzyl ether using a solvent-switching technique.
Simultaneous HPLC separation of the enantiomers of 3-benzyloxy-2-methyl-1,2-propanediol and the corresponding 3-benzyloxy-2-methyl-1,2-propene oxide could be accomplished on amylose derived Chiralpak AD switching between 10% 2-propanol and 3% 1,2-dimethoxyethane as polar modifier in n-heptane.
Steinreiber
A
A
Karl-Franzens University Graz, Institut für Chemie, Austria.
Strauss
U
U
Mayer
S F
SF
Uray
G
G
D002849:Chromatography, Gas / Q000379:methods; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D010647:Phenyl Ethers / Q000302:isolation & purification*; D013237:Stereoisomerism
C434546:2-methylglycerol-1-benzyl ether; C434547:2-methylglycidol-1-benzyl ether; D010647:Phenyl Ethers