title: Simultaneous direct high-performance liquid chromatographic enantioseparation of 2-methylglycidol-1-benzyl ether and 2-methylglycerol-1-benzyl ether using a solvent-switching technique.
abstract: Simultaneous HPLC separation of the enantiomers of 3-benzyloxy-2-methyl-1,2-propanediol and the corresponding 3-benzyloxy-2-methyl-1,2-propene oxide could be accomplished on amylose derived Chiralpak AD switching between 10% 2-propanol and 3% 1,2-dimethoxyethane as polar modifier in n-heptane.
authors: Karl-Franzens University Graz, Institut für Chemie, Austria.
authors: A
authors: A
authors: Steinreiber
authors: U
authors: U
authors: Strauss
authors: S F
authors: SF
authors: Mayer
authors: G
authors: G
authors: Uray
mesh_terms: D002849:Chromatography, Gas / Q000379:methods; D002851:Chromatography, High Pressure Liquid / Q000379:methods*; D010647:Phenyl Ethers / Q000302:isolation & purification*; D013237:Stereoisomerism
chemical_list: C434546:2-methylglycerol-1-benzyl ether; C434547:2-methylglycidol-1-benzyl ether; D010647:Phenyl Ethers